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Rules of thumb for chemical engineers / Stephen M. Hall

データ種別 電子ブック
著者標目 *Hall, Stephen author
出版者 (Amsterdam ; Cambridge, MA : Elsevier)
出版年 [2018]

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URL 図書館共通

EB007512
9780128110386 禁帯出

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Sixth edition.
巻次 ISBN:9780128110386
ISBN:0128110384
ISBN:9780128110379
ISBN:0128110376
大きさ 1 online resource
内容注記 Safety
Introduction
Process Safety Management (PSM)
Process Hazard Analysis (PHA)
Safe Design Practices
Emergency Vent Systems
Fire Outside the Vessel
Runaway Reaction
Blocked-In Line
Flash Point of Binary Mixtures
Deflagration Prevention or Control
Prevent Backflow
Equipment Purging
Dilution Purging
Displacement Purging
Pressure-Cycle Purging
Evacuation-Replacement Purging
Electrical Area Classification
Causes for Loss of Containment
Dust Explosion Hazards
References
Further Reading
Process Evaluation
Introduction
Accuracy of Cost Estimates
Definition of Scope
Treatment of Uncertainty and Contingency
User Requirements
Block Diagrams
Process Flow Diagrams (PFDs)
Basis of Design (BOD)
Block-Sequential Diagrams
Piping & Instrumentation Diagrams (P & IDs)
Factory Assembled Skids and Modules
Data Sheets and Specifications
Capital Cost Estimates
Organization of a Cost Estimate
Example of a Screening Estimate for a Refinery
Engineering
Reference
Process Modeling
Introduction
Concepts and Terminology
Equipment Design
Mass and Energy Transfer
Flow Sheet Simulation
Flow Sheet Simulation
Discrete Process Simulation
General Purpose Simulation Environments
Software List
References
Fluid Flow
Introduction
Data Required
Design Documents
Material and Energy Balance
Physical Properties of the Materials
General Procedure
Recommended Velocity
Compressible Flow of a Gas
Oil/Gas Mixtures
Check Valves
Equivalent Length
Shortcut Equation for Pressure Drop Due to Friction
Reynolds Number
Friction Factor
Surface Roughness
Incompressible Flow
Compressible Flow
Compressible Flow
Weymouth Equation
Panhandle A Equation
Panhandle B Equation
Compressible Flow
Visual Basic Subroutines for Pressure Drop Due to Friction
Reynolds Number
Darcy Friction Factor
Pressure Drop Due to Friction
Orifices
Incompressible Flow (Liquids)
Compressible Flow (Gases)
Control Valves
Water Hammer
Partially Full Horizontal Pipes
Two-Phase Flow
Lockhart-Martinelli
Homogeneous Model
Split Bounds Model
Asymptotic Model
Comparison of the Two-Phase Models
References
Further Reading
Vessels
Introduction
Cost Considerations
Safety Considerations
General Rules of Thumb for Vessels
Atmospheric Storage Tanks
Pressure Vessels and Reactors
Tank Dimensions
Liquid Volume at Any Fill Height
Time to Drain a Tank
Emissions From Storage Tanks
Load Cells
Liquid-Liquid Separators
Vapor-Liquid Separators
Liquid Surge Volume
Vapor Velocity in the Disengagement Section
Vapor-Liquid Separator Size
Vertical Separator
Horizontal Separator
Horizontal Drum With Water Separation
Vessel Specifications
Good Engineering Practices for Storage Tank and Vent Relief Design
References
Further Reading
Blending and Agitation
Introduction
Safety Considerations
Basics
Impeller Types
Dimensional Analysis
Reynolds Number and Turbulence
Pumping Number
Power and Power Number
Blending
Newtonian Fluids in Turbulent or Transitional Flow
Shear-Thinning Fluids
Laminar Flow Regime
Solids Suspension
Terminal Settling Velocity
Scale of Agitation
Number and Location of Impellers
Impeller Speed and Agitator Power
Gas Dispersion
In-Line Mixers
High-Shear Mixers
Mixing Solids
Mechanical Design
Torque
Shaft Diameter
Impeller Weight
Critical Speed
References
Further Reading
Pumps
Introduction
Safety Considerations
Pump Types and Selection
Centrifugal Pumps
Positive Displacement Pumps
Pump Specification Checklist
Good Design Practice
Pump Testing
System Curves
Sensitivity
Operating Point-and-Pump Selection
Flow Control With Throttling Valve
Control Valve
Charting Control Characteristics
Flow Control by Changing the Pump Speed
Affinity Laws
Power
Minimum Flow
Temperature Rise
Suction System NPSH Available
Suction System NPSH for Studies
Multiple Centrifugal Pumps in Parallel or Series
References
Further Reading
Fans, Blowers, and Compressors
Introduction
Safety Considerations
Rules of Thumb
Rules of Thumb (Compressors)
Good Engineering Practice
Compressed Air Systems
Fans
Fan Noise
Blower Types
Compressor Types
Surge Control
Performance Calculations
Definitions
Affinity Laws
Power
Power
Power
Comparison With Manufacturer's Data
Power With P-E Diagram
Cost of Compressed Air
Receiver Volume
Time to Pump System to Pressure
References
Further Reading
Vacuum Systems
Introduction
Safety Considerations
Vacuum Units
Conversion Between Mass Flow, Actual Volume Flow, and Standard Volume Flow
Comparison of Vacuum Equipment
Vacuum Jets
Liquid-Ring Vacuum Pumps
Correcting for Seal Liquid Temperature and Composition
Dry Vacuum Pumps
Typical Jet Systems
Steam Supply
Measuring Air Leakage
Time to Evacuate
Instrumentation and Controls
References
Further Reading
Pneumatic Conveying
Introduction
Safety Considerations
Flow Regimes
Types of Systems
System Design Procedure
Saltation Velocity
Pressure Drop
Pressure Drop of Carrier Gas
Acceleration of Solids
Friction of Solids in Straight Pipe
Friction of Solids in Elbows
Lifting of Solids Through Vertical Sections
Miscellaneous Factors
Prime Movers
Feed Systems
Silos
Conveyor Piping
Disengagement
References
Filtration
Introduction
Basket Strainers
Cartridge Filters
Vacuum Drum Filters
Filter Presses
Membrane Filters
References
Heat Exchangers
Introduction
Safety Considerations
TEMA
Selection Guides
Shell-and-Tube Heat Exchangers
Plate-and-Frame Heat Exchangers
Spiral Heat Exchangers
Helical Coil Heat Exchangers
Design Recommendations
Process Data
Heat Exchanger Configuration and Area
Determining the LMTD Configuration Correction Factor
Tube Side Pressure Drop
Tube Side Film Coefficient
Shell Diameter
Ideal Shell Side Film Coefficient
Shell Side Film Coefficient Correction Factors
Baffle Cut and Spacing, Jc
Baffle Leakage Effects, Jl
Bundle and Partition Bypass Effects, Jb
Variations in Baffle Spacing, Js
Temperature Gradient for Laminar Flow Regime, Jr
Overall Heat Transfer Coefficient
Shell Side Pressure Drop
Heat Transfer Coefficients
Fouling Resistances
Installation Recommendations
Thermal Conductivity of Metals
Vacuum Condensers
Air-cooled Heat Exchangers: Forced vs
Induced Draft
Air-Cooled Heat Exchangers: Air Data
Air-Cooled Heat Exchangers: Thermal Design
Air-Side Heat Transfer Coefficient
Air-cooled Heat Exchangers: Pressure Drop, Air Side
Air-Cooled Heat Exchangers: Temperature Control
References
Further Reading
Closed-Loop Heat Transfer Systems
Introduction
Safety Considerations
Selecting the Heat Transfer Fluid
Types of Heat Transfer Fluids
Heat Transfer Coefficient
System Design
Temperature Control
Case 1: Single-Temperature Central System
Case 2: Dual-Temperature Central System
Case 3: Three-Temperature Central System
Physical Properties of Commercial Heat Transfer Fluids
References
Fractionators
Introduction
Safety Considerations
Separation Factor
Relative Volatility
Vapor-Liquid Equilibrium (VLE)
Activity Coefficients
Sources for Activity Coefficients
Establishing the Column Pressure
Minimum Reflux
Bubble Point Liquid Feed
Dew Point Vapor Feed
Minimum Reflux
Minimum Stages
Relationship of Theoretical Stages to Reflux Ratio
Feed Location
Reflux-to-Feed Ratio
Actual Trays
Graphical Methods
Plotting With Murphree Tray Efficiency
Tray Efficiency Rules of Thumb
Using the McCabe-Thiele Plot
Column Internals
Column Tray Spacing
Tower Diameter
Pressure Drop
Control Schemes
Flow
Column Pressure
Level in the Overhead Receiver
Level in the Bottom of the Tower
Composition Control
Constraints
Reboilers
Packed Columns
References
Further Reading
Absorbers
Introduction
Safety Considerations
Hydrocarbon Absorber Design
Inorganic Absorbers
Packing Height for Mass Transfer in Packed Columns
Overall Mass Transfer Coefficient
References
Further Reading
Controls
Introduction
Basic Nomenclature
Definitions of Control Modes
Proportional Control
Integral (Reset) Control
Derivative Control
Cascade Control
Specifying Instruments to Measure Values
Control Ranges
Drawing Conventions
Artistic Expression
Safety Instrumented Systems
Enclosures: NEMA and IP
References
Further Reading
Biopharmaceutical Systems
Introduction
Facility Design and Sterilization Best Practices
General Design Considerations
System Design Considerations
CIP System Design Considerations
Sterilize (or Sanitize)-in Place (SIP) System Design Considerations
Disposable Systems
Disposable System Economic Evaluation
Disposable System Environmental Life Cycle Assessment
Open or Closed?
Contamination Root Causes
Design and Sterile Boundary Faults
Equipment Faults
Human Error (Procedures, Execution)
Contamination Investigation and Recovery
Time Is of the Essence
Go for Data
Widen the Search
Get Hands-On
Time to Open Up
Experimental
Microbiology Investigation
Risk Assessment
Validation
References
Further Reading
Bioprocessing
Introduction
Bioreactor Systems
Typical Geometric and Engineering Parameters
Bioreactor Controllers
Clean Gas Supply to Bioreactors
Oxygen Transfer
Heat Transfer
pH Control
Downstream Processes
Chromatography Purification
Buffer Prep
Liquid Waste Inactivation
References
Energy Conservation
Introduction
Calculating Steam Cost
Steam System Rules of Thumb
Equivalent Cost of Fuels
Steam Traps
Energy Efficient Design for Fractionators
Pinch Analysis
Insulation
References
Drivers
Introduction
Electric Motors
Motor Voltages
Motors: Efficiency
Motors: Starter Sizes
Motors: Useful Equations
Motors: Overloading
Air-Driven Motors
Hydraulic Motors
Steam Turbines: Steam Rate
Steam Turbines: Efficiency
Gas Turbines: Performance
Internal Combustion Engines: Fuel Rates
Gas Expanders: Available Energy
References
Boilers
Introduction
Boiler Horsepower
Types of Packaged Boilers
Power Plants
Controls
Thermal Efficiency
Stack Gas Enthalpy
Steam Drum Stability
Deaerator Venting
Water Alkalinity
Source Water Impurities
Conductivity Versus Dissolved Solids
Silica in Steam
Caustic Embrittlement
Waste Heat
Boiler Feedwater
Blowdown Control
Best Practices
References
Further Reading
Cooling Towers
Introduction
Safety Considerations
Mechanical Draft Cooling Towers
Material and Energy Balance Calculations
Rating Nomenclature
Performance Calculations
Operations and Accessories
Water Quality Guidelines
Scale Prevention
References
Refrigeration
Introduction
Specifications
Indirect and Direct System Design
Horsepower Per Ton
Refrigerants
Refrigerant Containment
Steam Jet Ejectors
Ammonia Absorption Utilities Requirements
Ammonia Heat Transfer Coefficient
References
Reliability
Introduction
Initial Design
Risk Analysis
Sustainable Practices
References
Further Reading
Metallurgy
Introduction
Cost Comparison
Embodied Energy
Embrittlement
Stress-Corrosion Cracking
Hydrogen Attack
Pitting Corrosion
Creep and Creep-Rupture Life
Naphthenic Acid Corrosion
Thermal Fatigue
Abrasive Wear
Pipeline Toughness
Common Corrosion Mistakes
References
Further Reading
Troubleshooting
Introduction
General Troubleshooting Approach
Diagnostic Tools
Instruments
Control Valves (Process Control)
Shell-and-Tube Heat Exchangers
Plate-and-Frame Heat Exchangers (PHEs)
Fractionation Towers
Fractionation Case Histories
Pinch
Key Components
Profiles
Troubleshooting Technique
Cutting Corners
Trapped Water
Cocurrent
Foaming
Stacking Packing
Tray Supports
Boilup Control
Condenser Velocity
Blind Blind
Temperature Control of Both Ends
Nozzle Bottleneck
Hatless Riser
Tilted Distributor
Hammer
Aeration
Siphoning
Hot-Vapor Rules Bypassed
Trapped
Centrifugal Pumps
Compressors
Steam Jet Vacuum Systems
Refrigeration
References
Further Reading
Startup
Introduction
Startup Management
Change Control During Startup
Startup Cost
Systems Approach
Construction Quality
Startup Checklists
Operating Modes
Normal Startup
Normal Operation
Normal Shutdown
Emergency Shutdown
Prolonged Shutdown
References
Conversion Factors and Constants
Significant Figures and Rounding
Gas Constant
Standard Gas Volume
Atmospheric Pressure
Irrigation Conversion
References
Properties
Introduction
Approximate Physical Properties
Vapor-Pressure Equation
Liquid Viscosity
Dynamic (or Absolute) Viscosity
Kinematic Viscosity
Viscosity of Mixtures
Emulsions
Saybolt Universal Seconds
Relative Humidity
Nomenclature
Surface Tension
Thermodynamic Properties of Water and Steam
Gas Diffusion Coefficients
Bulk Modulus
Water and Hydrocarbons
Water in Natural Gas
Hydrocarbons in Water
Methanol Injection
Compressibility Factor
Inorganic Gases in Petroleum
Foam Density
Equivalent Diameter
Estimating Equivalent Diameter of Solids
Properties Data Sheet
References
Further Reading
一般注記 Includes bibliographical references and index
Online resource; title from PDF title page (EBSCO, viewed November 1, 2017)
Rules of Thumb for Chemical Engineers, Sixth Edition, is the most complete guide for chemical and process engineers who need reliable and authoritative solutions to on-the-job problems. The text is comprehensively revised and updated with new data and formulas. The book helps solve process design problems quickly, accurately and safely, with hundreds of common sense techniques, shortcuts and calculations. Its concise sections detail the steps needed to answer critical design questions and challenges. The book discusses physical properties for proprietary materials, pharmaceutical and biopharmaceutical sector heuristics, process design, closed-loop heat transfer systems, heat exchangers, packed columns and structured packings. This book will help you: save time you no longer have to spend on theory or derivations; improve accuracy by exploiting well tested and accepted methods culled from industry experts; and save money by reducing reliance on consultants. The book brings together solutions, information and work-arounds from engineers in the process industry
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分 類 LCC:TP151
DC23:660
書誌ID OB00007512
ISBN 9780128110386

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